With the rapid development and complex challenges of chemical substances, new drug synthesis pathways are usually the most effective.24686-78-0,1-Benzoylpiperidin-4-one,as a common compound, the synthetic route is as follows.
REFERENCE EXAMPLE 10B In the same manner as in Reference Example 2B, omega-cyano-4-isopropoxy-3-methoxyacetophenone, 1-benzoyl-4-piperidone and sulfur were reacted to yield 2-amino-6-benzoyl-3-(4-isopropoxy-3-methoxybenzoyl)-4,5,6,7-tetrahydrothieno[2,3-c]pyridine, which was then recrystallized from ethyl acetate-hexane to yield yellow prismatic crystals having a melting point of 158 to 160 C., 24686-78-0
The synthetic route of 24686-78-0 has been constantly updated, and we look forward to future research findings.
Reference：
Patent; Takeda Chemical Industries, Ltd.; US6046189; (2000); A;,
Piperidine – Wikipedia
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