20845-34-5, 1-Methyl-2-piperidinemethanol is a piperidines compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
Synthesis of 2-(hydroxymethyl)-1-(2-isothiocyanatoethyl)-1-methylpiperidin-1-ium trifluoromethanesulfonate: A solution of 2-Isothiocyanatoethyl trifluoromethanesulfonate (30.2 mg, 0.128 mmol) and (1-methylpiperidin-2-yl)methanol (17.4 mg, 1.05 eq.) in toluene (0.5 mL) was stirred at RT for 2 hrs. The solvent was decanted and the residual oil was dissolved in DCM (0.3 mL) and Et2O (diethyl ether) (1 mL) was added to precipitate the salt. The top solvent layer was decanted. This process repeated twice. The residue was dried in high vacuum to give 41.9 mg (89.7percent) as colorless oil. MS-ESI: 129.84 (M-CH2CH2NCS?OTf?), 215.07 (M-OTf?), 20845-34-5
The synthetic route of 20845-34-5 has been constantly updated, and we look forward to future research findings.
Reference£º
Patent; The Procter & Gamble Company; GARCIA-GARCIA, Jose Carlos; HAZEN, Stanley Leon; WOS, John August; (43 pag.)US2017/152222; (2017); A1;,
Piperidine – Wikipedia
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