Chemistry is the experimental and theoretical study of materials on their properties at both the macroscopic and microscopic levels.In a patent， Quality Control of: tert-Butyl piperidin-4-ylcarbamate, Which mentioned a new discovery about 73874-95-0
The invention discloses a process for preparing 4 – Boc – amino piperidine method, comprises the following steps: N – benzyl – 4 – piperidone in under the acid catalysis with orthoformate in alcoholic solution react to form a ketal, then with the tert-butyl carbamate reaction of the imine, then imine by Pd/C catalytic hydrogenation reduction to obtain 4 – Boc – amino piperidine. The method the synthetic route is brief, raw materials are easy, low cost, simple and convenient operation, the reaction yield is high, product separation and purification, it has very good application prospect. (by machine translation)
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Reference：
Piperidine – Wikipedia,
Piperidine | C5H14020N – PubChem