85908-96-9, N-Boc-2-Piperidone is a piperidines compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
85908-96-9, Diisopropylamine (1.7 mL, 12.1 mmol) of THF (10 mL)To the solution was added n-butyllithium (6.7 ml, 11.0 mmol) was added dropwise at -78 C., and the mixture was stirred for 30 minutes. Compound 34 (2 g, 10.0 mmol) in THF (10 mL) was added dropwise, and the mixture was stirred for 15 minutes. A solution of N-tert-butylbenzenesulfinimidoyl chloride (2.6 g, 12.1 mmol) in THF (5 mL) was added and the mixture was stirred for 30 minutes. Water was added to the reaction solution, the mixture was extracted with ethyl acetate, dried over anhydrous sodium sulfate, and concentrated under reduced pressure. The resulting residue was purified by silica gel chromatography (hexane / ethyl acetate) to give Compound 35 (750 mg, yield: 38%) as an orange solid.
The synthetic route of 85908-96-9 has been constantly updated, and we look forward to future research findings.
Reference：
Patent; THE UNIVERSITY OF TOKYO; TOHOKU UNIVERSITY; SHIONOGI & COMPANY LIMITED; NAGANO, TETSUO; OKABE, TAKAYOSHI; KOJIMA, HIROTATSU; KAWAGUCHI, MITSUYASU; NUREKI, OSAMU; ISHITANI, RYUICHIRO; NISHIMASU, HIROSHI; AOKI, JUNKEN; TANAKA, NOBUYUKI; TATENO, YUSUKE; TAKAHASHI, YU; (85 pag.)JP2016/193887; (2016); A;,
Piperidine – Wikipedia
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