Simple exploration of 63295-48-7

Here is a brief introduction to this compound(63295-48-7)Reference of Iron(III) trifluoromethanesulfonate, if you want to know about other compounds related to this compound(63295-48-7), you can read my other articles.

Reference of Iron(III) trifluoromethanesulfonate. The protonation of heteroatoms in aromatic heterocycles can be divided into two categories: lone pairs of electrons are in the aromatic ring conjugated system; and lone pairs of electrons do not participate. Compound: Iron(III) trifluoromethanesulfonate, is researched, Molecular C3F9FeO9S3, CAS is 63295-48-7, about Clean production of ethyl levulinate from kitchen waste. Author is Tian, Lu; Zhang, Luxin; Liu, Yuting; He, Yunfei; Zhu, Yujie; Sun, Ruijun; Yi, Simin; Xiang, Junping.

A clean and highly efficient catalytic system for the synthesis of Et levulinate (EL) from kitchen waste was developed. A heterogeneous catalyst (Sn/ZrP-SO3H) was prepared and the Bronsted and Lewis acid sites on the surface of the catalyst were evaluated by pyridine FT-IR. Other physicochem. properties were also characterized using XRD, SEM, FT-IR, XPS, BET, NH3-TPD. The yield of EL obtained was 49.27%, when glucose was used as the starting material and subjected to 170°C for 10 h in the presence of the solid acid catalyst, Sn/ZrP-SO3H. The prepared catalyst was also combined with several metal triflates; (Al(OTf)3, Fe(OTf)3, Sm(OTf)3) to form a catalytic system for the efficient preparation of EL from kitchen waste. Sn/ZrP-SO3H/Al(OTf)3 had superior activity compare to other catalyst combinations. In single factor experiments, the yield of EL reached 52.52% after heating at 170°C for 4 h. In addition, four-factor and three-level experiments were performed using response surface methodol. (RSM) to analyze the interaction between each factor. The optimal reaction conditions predicted by the model (163°C, 7.63 h, 20 mg Al(OTf)3, 40 mg Sn/ZrP-SO3H and 79.98 mg of kitchen waste) estimated a maximal yield for EL of 51.24%. The exptl. yield of EL however was 52.03% which confirms the reliability of the model. This work provides a cleaner production technol. for the synthesis of the high value-added chem. EL, and a sustainable route for the utilization of kitchen waste.

Here is a brief introduction to this compound(63295-48-7)Reference of Iron(III) trifluoromethanesulfonate, if you want to know about other compounds related to this compound(63295-48-7), you can read my other articles.

Reference:
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