14813-01-5, 1-Benzylpiperidin-3-ol is a piperidines compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
1000ml three bottles, a solution of D-CSA (58 g, 0.25 mol) in 116 ml of isopropanol was added dropwise to 478 ml of isopropanol, and the mixture was stirred at room temperature for 1 hour to precipitate a solid. 0 C for 2 hours, filtered, washed with cold isopropanol (30 ml) and dried to give 75 g of (R) -1-benzyl-3-hydroxypiperidine camphorsulfonate. (Ee: 95%) (theory: 105.9 g). (R) -1-benzyl-3-hydroxypiperidine camphorsulfonate having a 95% ee value was recrystallized from 3-fold amounts of isopropanol to give (R) -1-benzyl- Camphorsulfonate (99% ee)., 14813-01-5
The synthetic route of 14813-01-5 has been constantly updated, and we look forward to future research findings.
Reference：
Patent; ABA Chemicals Corporation; Lin, ZhiGang; Xu, Jun; Liu, YanQin; Que, limin; Jiang, yueheng; CAI, Tong; (13 pag.)CN103864673; (2016); B;,
Piperidine – Wikipedia
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