14813-01-5, 1-Benzylpiperidin-3-ol is a piperidines compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
Step 1: To a stirred solution of [5] (2.0g, 10.47mmol), vinyl acetate (10.0ml, lOO.Ommol) was added at room temperature. After an additional stirring for 5 minutes at same temperature, PS-IM (0.20g, 10%) was added. The reaction temperature was allowed to increase up to 40C and stirring was continued for 16 h. Reaction mixture was passed through the bed of celite and evaporated to dryness which was further purified using silica gel column chromatography using 10% ethyl acetate/hexane as eluent to afford [6](0.9g, 45%)and [7] (0.8g, 40%) as transparent sticky material. Analytical Data: [6] ESIMS: 192 [M++1][7]ESIMS: 234 [M++l]., 14813-01-5
The synthetic route of 14813-01-5 has been constantly updated, and we look forward to future research findings.
Reference：
Patent; SPHAERA PHARMA PVT. LTD.; DRUG DISCOVERY RESEARCH CENTRE; DUGAR, Sundeep; MAHAJAN, Dinesh; RAI, Santosh Kumar; RAO, Kanury; SINGH, Varshneya; WO2015/181837; (2015); A2;,
Piperidine – Wikipedia
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