10315-06-7, Methyl 1-benzylpiperidine-4-carboxylate is a piperidines compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
Preparation of V-2 A solution of V-l (20 g, 85.72 mmol) in 80 mL of THF (dry) was added dropwise over lh to a solution of LDA (60 mL, 2.0 M, 120 mmol) in 80 mL of THF (dry) at 0C. The resultant mixture was stirred at 0C for 30 min, and then added to a pre-cooled (0C) solution of N- fluorobenzenesulfonimide (28.38 g, 90 mmol) in 120 mL of THF (dry). The resulting reaction mixture was stirred at 0C for 30 min, and then at 25C overnight. After dilution by 400 mL of EtOH, the mixture was washed with water (100 mL x3) and brine (100 mL), dried and concentrated. The crude was purified by silica gel chromatography (PE to PE/DCM=2/1 to DCM to DCM/MeOH=200/l) to afford V-2 (6 g, yield: 28%) as a colorless oil., 10315-06-7
The synthetic route of 10315-06-7 has been constantly updated, and we look forward to future research findings.
Reference：
Patent; SUZHOU SHANGZHI BIOTECH LIMITED; CHENG, Xueheng; WO2014/8629; (2014); A1;,
Piperidine – Wikipedia
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