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Reference of 236406-39-6, The reaction rate of a catalyzed reaction is faster than the reaction rate of the uncatalyzed reaction at the same temperature.236406-39-6, Name is 8-Boc-2,8-Diazaspiro[4.5]decane, molecular formula is C13H24N2O2. In a Article£¬once mentioned of 236406-39-6

The synthesis of closo- and nido-(aminoalkyl)dicarbaboranes: A re-examination of contradictory literature reports, crystal structure of [7-{H3N(CH2)3}-7,8-C2B9H 11]¡¤NH2NH2

The reaction of Li[1-tBuMe2Si-1,2-C2B10H10 ] with N-(bromoethyl)phthalimide or N-3-(bromopropyl)phthalimide generates unusual carboranyl heterocycles, resulting from nucleophilic substitution followed by insertion of a phthalimide carbonyl into the C-Si bond. The structure of one was determined by single crystal X-ray diffraction. Reaction of the heterocycles with nBu4NF affords closo-1-{C6H4(CO)2N(CH2)n }-1,2-C2B10H11 (1b n = 2 and 1c n = 3) together with the anions nido-[7-{C6H4(CO)2N(CH2)n }-7,8-C2B9H11]- as minor side-products on prolonged reaction. The prolonged reaction of 1b and 1c with hydrazine results in deboronation to give hydrazine solvates of zwitterionic nido-[7-{H3N(CH2)n}-7,8-C2B9 H11]. A single crystal X-ray diffraction study for one reveals an elegant dimeric architecture supported by hydrazine-bridged hydrogen bonds. The reaction of the heterocycles with ethanolic KOH results in cluster deboronation and partial deprotection of the amine group to give nido-[7-(2-O2CC6H4CONH)-(CH2)n -7,8-C2B9H11]2- as potassium salts which can be metathesised to less hygroscopic Me3NH+ salts. The molecular structure of one of the latter displays hydrogen bonding generating a dimeric unit. Complete deprotection of the amine function in these salts by water-HCl gives zwitterionic aminoalkylcarboranes nido-7-{H3N(CH2)n}-7,8-C2B9 H11.

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Reference£º
Piperidine – Wikipedia,
Piperidine | C5H19379N – PubChem