79099-07-3, 1-Boc-4-Piperidone is a piperidines compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
79099-07-3, In a reaction flask, 20 g (0.1 mol) of N-Boc-4-piperidone was added to 200 mL of toluene,Then 18 g (0.2 mol) of dimethyl carbonate and 22 g (0.2 mol) of potassium tert-butoxide were added, and the mixture was heated to 70 ¡ã C. for 1 hour,Cooled to room temperature, quenched with water 100mL,The reaction solution was adjusted to pH 7 with 1 mol / L HCl,Extracted with ethyl acetate, dried over anhydrous sodium sulfate,Dried to give N-Boc-3-methyl-4-piperidone as a yellow oil 25 g;
The synthetic route of 79099-07-3 has been constantly updated, and we look forward to future research findings.
Reference£º
Patent; Wang Erxia; (19 pag.)CN107266442; (2017); A;,
Piperidine – Wikipedia
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