54012-73-6,54012-73-6, Piperidin-3-amine is a piperidines compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
The steps will be a 3 – amino piperidine (50.1g) soluble in the 2L of in DMF, by adding 1, 2 – diphenyl vinylidene carbonate (119.1g), triethylamine (1L), for ice water bath stirring to the reaction is complete (about 30min) after, adding ethyl acetate, the combined organic layer, dried with anhydrous sodium sulfate, to remove the organic solvent. The resulting product is dissolved in the 1L trifluoroacetic in, as for 20 C stirring for 2 hours, concentrated in vacuo, to remove the surplus trifluoro acetic acid, to obtain a product of formula Chinese (148.5g, yield 92.3%)
The synthetic route of 54012-73-6 has been constantly updated, and we look forward to future research findings.
Reference£º
Patent; Borui Bio-pharmaceutical (Suzhou) Co., Ltd.; Yuan Jiandong; (12 pag.)CN103450201; (2017); B;,
Piperidine – Wikipedia
Piperidine | C5H11N – PubChem