1211587-42-6, Benzyl 4-((chlorosulfonyl)methyl)piperidine-1-carboxylate is a piperidines compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
Compound 13 was prepared from sulfochloride 11 analogously to 12. Yield 11.6g (63%). White solid. Mp 75-76. [alpha]D=+5.3 ( 1.03, MeOH). MS (CI, m/z): 502 (MH+). Anal. Calcd for C26H35N3O5S: C, 62.25; H, 7.03; N, 8.38; S, 6.39. Found: C, 61.87; H, 7.09; N, 8.21; S, 6.48. 1H NMR (500MHz, CDCl3) delta 7.52-7.29 (m, 7H), 7.29-7.20 (m, 3H), 6.08-5.80 (m, 1H), 5.66-5.30 (m, 1H), 5.12 (s, 2H), 4.10 (s, 2H), 4.04-3.91 (m, 2H), 3.21-3.11 (m, 1H), 3.04-2.93 (m, 1H), 2.75 (s, 2H), 2.53-2.37 (m, 2H), 2.03-1.87 (m, 1H), 1.83-1.65 (m, 2H), 1.12 (d, J=6.0Hz, 3H), 1.12-1.04 (m, 2H), 1.04 (d, J=6.1Hz, 3H). 13C NMR (126MHz, cdcl3) delta 169.6, 155.1, 136.7, 136.6, 129.6, 128.9, 128.5, 128.0, 127.8, 127.4, 67.1, 59.0, 58.6, 43.6, 41.8, 39.4, 31.7, 31.5, 22.5, 22.3.
1211587-42-6, 1211587-42-6 Benzyl 4-((chlorosulfonyl)methyl)piperidine-1-carboxylate 50988934, apiperidines compound, is more and more widely used in various fields.
Reference：
Article; Grygorenko, Oleksandr O.; Zhersh, Sergey; Oliinyk, Bohdan V.; Shishkin, Oleg V.; Tolmachev, Andrey A.; Tetrahedron Asymmetry; vol. 25; 3; (2014); p. 229 – 237;,
Piperidine – Wikipedia
Piperidine | C5H11N – PubChem