896464-16-7, tert-Butyl 2,7-diazaspiro[3.5]nonane-7-carboxylate is a piperidines compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
In a microwave vessel, a mixture of tert-butyl 2,7-diazaspiro[3 .5 ]nonane-7-carboxylate (85 mg, 0.38 mmol), DIEA (44 jiL, 0.25 mmol), and 4-(6-fluoropyridin-3-yl)-6-(i-methyl-1H- pyrazol-4-yl)pyrazolo[i,5-a]pyridine-3-carbonitrile (Intermediate P6; 40 mg, 0.13 mmol) in DMSO (1 mL) was subjected to microwave irradiation at 125 C for 2 h. After cooling to ambient temperature, the reaction mixture was directly purified by reverse-phase preparative HPLC (10 to 80% acetonitrile/water) to give the title compound (12 mg, 18% yield). MS (apci) m/z = 525.2 (M+H)., 896464-16-7
896464-16-7 tert-Butyl 2,7-diazaspiro[3.5]nonane-7-carboxylate 24820512, apiperidines compound, is more and more widely used in various fields.
Reference£º
Patent; ARRAY BIOPHARMA, INC.; ANDREWS, Steven W.; BLAKE, James F.; CHICARELLI, Mark J.; GOLOS, Adam; HAAS, Julia; JIANG, Yutong; KOLAKOWSKI, Gabrielle R.; (594 pag.)WO2017/11776; (2017); A1;,
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