Category: 181269-69-2

181269-69-2, tert-Butyl 3-methyl-4-oxopiperidine-1-carboxylate is a piperidines compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated

To a solution of compound 3 (11.00 mmol) in ethanol (50 mL) was added KBH4 (0.712 g, 13.20mmol) slowly at 0 C . The reaction mixture was stirred at 0 Cfor 0.5 h and the stirred at RT for 2 h. The reaction mixture was pure into water (50 mL) and extracted with DCM (50 mL3). The organic layer was dried and concentrated to give the product, 181269-69-2

The synthetic route of 181269-69-2 has been constantly updated, and we look forward to future research findings.

Reference£º
Patent; NOVIRA THERAPEUTICS, INC.; HARTMAN, George D.; FLORES, Osvaldo A.; WO2013/96744; (2013); A1;,
Piperidine – Wikipedia
Piperidine | C5H11N – PubChem

181269-69-2, tert-Butyl 3-methyl-4-oxopiperidine-1-carboxylate is a piperidines compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated

NaBH4 (2.18 g, 57.7 mmol) was added to a solution of compound 27B (6.10 g, 28.8 mmol) in ethanol (200 ml) at 0 C. over a period of 20 min. After 30 min, the reaction mixture was concentrated. EtOAc (150 ml) was added, and the mixture was washed with brine, dried (Na2SO4), filtered, and concentrated to provide 5.45 g (25.5 mmol, 88%) of compound 38 as a colorless oil. MS: m/e 160 (M-56).

181269-69-2, 181269-69-2 tert-Butyl 3-methyl-4-oxopiperidine-1-carboxylate 22644642, apiperidines compound, is more and more widely used in various.

Reference£º
Patent; SCHERING CORPORATION; US2005/182095; (2005); A1;,
Piperidine – Wikipedia
Piperidine | C5H11N – PubChem