167414-75-7, Benzyl 4-(3-ethoxy-3-oxopropanoyl)piperidine-1-carboxylate is a piperidines compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
167414-75-7, Intermediate 5, 3.8 g (20 mmol), intermediate 3 7.99 g (24 mmol) was added to a 50 mL round bottom flask. Add 20 mL of acetic acid to dissolve, and react at 130 ¡ãC overnight. After the reaction is completed, the acetic acid is removed by rotary evaporation. 1M NaOH was added dropwise to precipitate a large amount of off-white solid, which was filtered. Washing with a small amount of MeOH gave a white solid M086. Yield 75.0percent.
The synthetic route of 167414-75-7 has been constantly updated, and we look forward to future research findings.
Reference£º
Patent; Kunming Xianghao Technology Co., Ltd.; Luo Huairong; Hong Xuechuan; Zhu Xi; Zhu Jinmei; Wu Guisheng; Deng Zixin; Zhu Yingmin; Lu Yungang; Deng Ke; Qu Chunrong; (25 pag.)CN103694242; (2016); B;,
Piperidine – Wikipedia
Piperidine | C5H11N – PubChem