1023301-84-9, tert-Butyl 2,7-diazaspiro[3.5]nonane-7-carboxylate hydrochloride is a piperidines compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
Take 4-trifluoromethoxybenzyl alcohol (85 mg, 0.44 mmol, 1.1 eq.).N,N’-carbonyldiimidazole (77 mg, 0.48 mmol, 1.2 eq.)In a 25 mL single-mouth bottle, DMF was dissolved and stirred at room temperature for 2 h.Compound 2-7 (105 mg, 0.4 mmol) was dissolved in DMF.Add triethylamine (64 muL, 0.48 mmol, 1.2 eq.),The reaction solution was added and stirred at room temperature. TLC tracking monitoring.The oil pump was rotated to remove most of the solvent, and EA and saturated sodium bicarbonate solution were added, washed with saturated brine, dried, dried, and passed through a column (PE: EA = 2:1). A white powder of 130 mg was obtained in a yield of 73%., 1023301-84-9
As the paragraph descriping shows that 1023301-84-9 is playing an increasingly important role.
Reference£º
Patent; Guangzhou Hengnuokang Pharmaceutical Technology Co., Ltd.; Zhang Jiancun; Lin Cai; Zou Qingan; (45 pag.)CN108456208; (2018); A;,
Piperidine – Wikipedia
Piperidine | C5H11N – PubChem