Related Products of 600-05-5. The fused heterocycle is formed by combining a benzene ring with a single heterocycle, or two or more single heterocycles. Compound: 2,3-Dibromopropionic acid, is researched, Molecular C3H4Br2O2, CAS is 600-05-5, about Selective detection of unknown organic bromine compounds and quantification potentiality by negative-ion electrospray ionization mass spectrometry with induced in-source fragmentation. Author is Huetteroth, Alexandra; Putschew, Anke; Jekel, Martin.
For the detection of unknown organic bromine compounds, a liquid chromatog.-mass spectrometry (LC-MS) method with neg.-ion electrospray ionization (NI-ESI) and induced in-source fragmentation (IISF) was established. After LC separation, the mols. are fragmentized in the source, and bromide is detected via m/z 79 and m/z 81 based on the isotopic occurrence of bromine. In this way, the retention times of the unknown organobromine compounds are determined, and this can be used to extract addnl. structural information (number of bound bromine atoms, mol. mass and fragmentation scheme) from measurements in the commonly used but less sensitive scan mode. The anal. of known organobromine compounds shows that LC/NI-ESI-IISF mass spectrometry with detection of m/z 79 and 81 is more sensitive than the detection of daughter ions (LC/ESI/MS-MS). Therefore, the authors present a method not only for the detection of unknown organic bromine compounds, but also for the selective and sensitive detection and quantification of known organobromine compounds
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