122860-33-7, Benzyl 4-(hydroxymethyl)piperidine-1-carboxylate is a piperidines compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
Triphenylphosphine (7.87 g, 30 mmol) and imidazole (2.05 g, 30 mmol, 1.5 equiv) in DCM at 0 0C under Ar was treated with I2 (7.61 g, 30 mmol, 1.5 equiv). After 5 min, benzyl 4-(hydroxymethyl)tetrahydro-l(2H)-pyridinecarboxylate (5.00 g, 20 mmol) in DCM was added. The reaction was stirred for 1 h and then quenched with 10% HCl. The reaction mixture was extracted with EtOAc and the organic layer was washed with NuaHCO3(sat). The organics were dried with NaCl(sat) and Na2SO4(s) and then removed under reduced pressure. The residue was then purified by column chromatography utilizing an ISCO system (EtOAc- hexane) to give 6.20 g (86%) of a white solid; m/z 360., 122860-33-7
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Reference：
Patent; ASTRAZENECA AB; ASTRAZENECA UK LIMITED; WO2006/24834; (2006); A1;,
Piperidine – Wikipedia
Piperidine | C5H11N – PubChem