In 2019 ORG BIOMOL CHEM published article about N-HETEROCYCLIC CARBENES; ARYL CHLORIDES; MECHANOCHEMISTRY; COMPLEXES; PRECATALYST; CATALYSTS; LIGANDS; NHC in [Cao, Qun; Nicholson, William I.; Jones, Andrew C.; Browne, Duncan L.] Cardiff Univ, Sch Chem, Main Bldg,Pk Pl, Cardiff CF10 3EQ, S Glam, Wales in 2019, Cited 35. The Name is 1,4-Dioxa-8-azaspiro[4.5]decane. Through research, I have a further understanding and discovery of 177-11-7. Recommanded Product: 177-11-7
An operationally simple mechanochemical method for the Pd catalysed Buchwald-Hartwig amination of arylhalides with secondary amines has been developed using a Pd PEPPSI catalyst system. The system is demonstrated on 30 substrates and applied in the context of a target synthesis. Furthermore, the performance of the reaction under aerobic conditions has been probed under traditional solution and mechanochemical conditions, the observations are discussed herein.
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