876378-16-4,876378-16-4, (S)-Benzyl 3-aminopiperidine-1-carboxylate hydrochloride is a piperidines compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
Oxalyl chloride (1.50 mL, 0.0177 mol) was added to 4-oxoadamantane-l-carboxylic acid (583 mg, 0.00300 mol) in methylene chloride (10 mL) at rt followed by 2 drops of DMF. The mixture was stirred at rt for 2 h. The volatiles were evaporated under reduced pressure and the residue was azeotropically evaported with toluene twice. The residue was dissolved in DCM (10 mL) and to the solution was added benzyl (3iS)-3-aminopiperidine-l-carboxylate hydrochloride (812.6 mg, 0.003001 mol) and A^Af-diisopropylethylamine (1.20 mL, 0.00689 mol). The mixture was stirred at rt for 1 h. The reaction mixture was diluted with DCM (100 mL) and washed with water, IN HC1 and brine. The organic phase was dried over NaiS04, filtered and concentrated to give the desired product.
876378-16-4 (S)-Benzyl 3-aminopiperidine-1-carboxylate hydrochloride 86605313, apiperidines compound, is more and more widely used in various fields.
Reference：
Patent; INCYTE CORPORATION; WO2006/20598; (2006); A2;,
Piperidine – Wikipedia
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