3612-20-2, 1-Benzylpiperidin-4-one is a piperidines compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
Step 1: Treat N-benzyl-piperidone (8.00 g, 0.0423 mol) in CH2Cl2 with (CH3)3SiCN (4.82 g, 0.0486 mol) and ZnI2 (0.68 g, 0.0021 mol). Stir at 23 C for 16 h and concentrate. Add CH3OH saturated with NH3 (30 mL) and heat at 40 C. Concentrate the resulting mixture, add CH2Cl2 (200 mL), dry (MgSO4), filter and concentrate to give 11.06 g of the desired product as a yellow oil. MS (Cl/CH4): m/e 189 (M-26).
3612-20-2, 3612-20-2 1-Benzylpiperidin-4-one 19220, apiperidines compound, is more and more widely used in various fields.
Reference：
Patent; SCHERING CORPORATION; EP1032561; (2004); B1;,
Piperidine – Wikipedia
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