Electric Literature of 309956-78-3, The reaction rate of a catalyzed reaction is faster than the reaction rate of the uncatalyzed reaction at the same temperature.309956-78-3, Name is (R)-tert-Butyl piperidin-3-ylcarbamate, molecular formula is C10H20N2O2. In a Patent，once mentioned of 309956-78-3
A advantage Geleg sandbank industrial production method. In accordance with the molar ratio of the 8 […] -7 the […] (the 2 butyne […] ) – 3 the the methylxanthines […] the 2 […] methyl -4 the quinazoline methyl […] added to a dipolar aprotic organic solvent, then adding alkali and potassium iodide, crystallization, filtration dried to obtain the intermediate I; the intermediate body in accordance with the molar ratio of the I (R) – 3 the […] butoxycarbonyl amino piperidine is added to a dipolar aprotic organic solvent, then adding alkali, crystallization, filtration washing remove the inorganic salt, to remove solvent under reduced pressure to obtain crude products, after methanol and isopropanol crystallization get midbody II; than the intermediate II according to the volume of the deprotection reagent, by adding to the reaction solvent, a crystallization to obtain crude products, then recrystallized with ethanol, filter to obtain final product advantage Geleg sandbank. The method of the invention can greatly shorten the production cycle, save the production cost, can be high purity, impurity removing effect is better, the method is safe and reliable, is simple and easy to operate, has good repeatability. (by machine translation)
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Reference：
Piperidine – Wikipedia,
Piperidine | C5H13515N – PubChem