31140-42-8, 3-Boc-Amino-2,6-dioxopiperidine is a piperidines compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
To a solution of tert-butyl (2-78, 2,6-dioxopiperidin-3-yl)carbamate (1.0 g, 4.38 mmol) in THF (15 mL) was added NaH (263 mg, 6.57 mmol) at 0 C. After stirring for 20 minutes at room temperature, iodomethane (327 muL, 5.26 mmol) was added to the reaction mixture. After stirring for 2 hours, the mixture was diluted with EtOAc and quenched with water. The organic layer was collected and the aqueous layer was washed with EtOAc. The combined organic layers were dried over Na2SO4, filtered and concentrated. The crude compound 2-79 was carried forward in the next step without additional purification., 31140-42-8
The synthetic route of 31140-42-8 has been constantly updated, and we look forward to future research findings.
Reference£º
Patent; DANA FARBER CANCER INSTITUTE, INC.; GRAY, Nathanael; JANG, Jaebong; DE CLERCQ, Dries; ECK, Michael; (201 pag.)WO2017/185036; (2017); A1;,
Piperidine – Wikipedia
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